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Status of NE-CAT Sector 24 ActivitiesJanuary 2008
APS accelerator operation was shut down for preventative maintenance for the month of January. Consequently there is no beamline user experience to report. The month long shut down presented an opportunity for the NE- CAT staff to perform preventative maintenance on the beamlines as well as introduce new capabilities for the users upon resumption of APS’ user operation in February. The major new capability introduced during the shut down was the installation of a sample placement robotic system on the 24-ID-C variable energy beam line. A photograph of the current installation is shown below.
The robotic system is an originally ALS designed and fabricated system which NE- CAT previously operated on its 8-BM bending magnet beamline. This beamline has been taken out of service and is in the process of being moved to Sector 24. In order to install the robot on to the 24-ID-C beamline extensive modifications were made. The “handedness” of the robot had to be reversed, i.e., looking downstream from the source, the robot had to be installed on the left side of the goniometer rather than the right as was the case of the 8-BM beam line. In performing this change all the electrical wiring and pneumatic tubing were upgraded to provide improved reliability. A new cover for the liquid nitrogen Dewar was also installed to minimize frosting and a gravity-feed liquid-nitrogen delivery system was installed to eliminate turbulence in the liquid nitrogen Dewar containing the samples during automatic filling. The operating software has also been integrated into the beamline data acquisition system. The end result of these many changes is that the robot can now operate unattended for several days mounting and dismounting sample pins hundreds of time without a failure. The first user test of the robot will take place in mid February. If the early user experiences are successful, the robot system will increasingly be scheduled for use by the user community.
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Recent Highlights08/19/2008 July-August status report now available. 7/07/2008 June status report now online. 06/24/2008 NE-CAT Hires Three New User Support Staff (More Info)
06/12/2008 May status report is now available. 05/06/2008 NE-CAT organizes a successful workshop titled “Software for Challenging Cases in Macromolecular Crystallography” at APS User Week 2008. A photo of the organizers and speakers is shown. Presentations can be found here. 4/04/2008 Featured Publication Crystal Structure of a Self-Spliced Group ll Intron Navtej Toor, Kevin S. Keating, Sean D. Taylor, and Anna Marie Pyle Science 4 April 2008, Vol. 320. No. 5872, pp. 77-82 04/01/2008 With the success users have had using the MD2 Microdiffractometer on 24-ID-E, NE-CAT is acquiring a second MD2 for 24-ID-C, delivery October 2008 2/27/2008 NE-CAT hosting the workshop “WK04, Software for Challenging Cases in Macromolecular Crystallography” to be held May 6, 2008 at APS User Week. See the APS User Meeting Website 1/22/2008 Modified ALS sample placement robotic system installed on 24-ID-C beamline Resource Advisory Committee Meeting Held NE-CAT Director Steven Ealick Provides Introductory Overview 16x16x300 micron crystal irradiated at 5 different positions using a 20 micron beam with the MD2 microdiffractometer to obtain a complete data set with a radiation-damage sensitive crystal First Data Frames Obtained Using the MD2 Microdiffractometer (see additional pictures) MD2 Microdiffractometer Installed on 24-ID-E beamline 5/22/2006 Phase 2 Vertical Focusing Mirror in Place. |
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